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Beilstein J. Org. Chem. 2018, 14, 2931–2939, doi:10.3762/bjoc.14.272
Graphical Abstract
Scheme 1: 1-Octene metathesis reaction.
Figure 1: A,B,C,D: XRD patterns of parent supports and catalysts used. Asterisk marks MoO3.
Figure 2: Conversion vs time curves for 1-octene metathesis over 6MoO3/MCM-22(28) and 6MoO3/SBA-15. Neat 1-oc...
Figure 3: Conversion vs time curves for the 1-octene metathesis over 6MoO3/MCM-56(13). Neat 1-octene, 1-octen...
Figure 4: Conversion vs time curves for 1-octene metathesis over 6MoO3/2D-MFI(26) and 6MoO3/HZSM-5(25). Neat ...
Figure 5: Conversion to oligomers for 1-octene over MCM-22(28) and MCM-22(70) (a) and conversion to oligomers...
Beilstein J. Org. Chem. 2015, 11, 2087–2096, doi:10.3762/bjoc.11.225
Figure 1: Hoveyda–Grubbs type catalysts used for immobilization.
Scheme 1: RCM of (−)-β-citronellene (1) and N,N-diallyl-2,2,2-trifluoroacetamide (2).
Figure 2: Conversion vs time dependence for RCM of (−)-β-citronellene over HGIIN+Cl−/MCM-36 (●), HGIIN+Cl−/SB...
Figure 3: Conversion vs. time dependences for RCM of DAF over catalysts HGIIN+Cl−/MCM-22 (▲), HGIIN+Cl−/MCM-5...
Figure 4: Splitting test for HGIIN+Cl−/MCM-56 in RCM of (−)-β-citronellene. Toluene, 60 °C, molar ratio (−)-β...
Figure 5: Self-metathesis of methyl oleate over HGIIN+Cl−/SBA-15 (■), HGIIN+Cl−/MCM-22 (▲), HGIIN+Cl−/MCM-56 ...
Scheme 2: Cross-metathesis of methyl oleate with cis-3-hexenyl acetate.
Figure 6: Conversion curves for CM of methyl oleate (full symbols) with cis-3-hexenyl acetate (open symbols) ...
Beilstein J. Org. Chem. 2011, 7, 22–28, doi:10.3762/bjoc.7.4
Figure 1: Grubbs 1 and Hoveyda–Grubbs 2 catalysts.
Figure 2: Zhan catalyst-1B.
Scheme 1: Metathesis reactions studied.
Figure 3: Conversion curves for the RCM of DEDAM with 3 in CH2Cl2 (open squares), 3/SBA-15 in CH2Cl2 (inverte...
Figure 4: Filtration experiments with 3/SBA-15. RCM of DEDAM in benzene (circles), 1,7-octadiene in cyclohexa...
Figure 5: Metathesis of methyl oleate (open symbols) and methyl 10-undecenoate (filled symbols) with 3/MCM-41...
Figure 6: UV–vis spectra of 3/SBA-15 (curve 2) and of 3 (curve 1) in dichloromethane (c = 0.001 mol/L, l = 0....
Figure 7: Spectra of the Ru 3d–C 1s photoelectrons for neat compound 3 (1), catalyst sample 3/SBA-15 (2) and ...